SYNTHESIS AND MODIFICATION OF THIN NASICON SOLID ELECTROLYTES USING ION BEAMS

1 CECCIO G.
Co-authors:
1 VACIK J. 2 MASTRONARDO I. 2 D’URSO C. 1 ŠTĚPANOVSKÁ E. 1 MIKŠOVÁ R.
Institutions:
1 Department of Neutron and Ion Methods, Nuclear Physics Institute of CAS, Hlavni 130, 250 68 Řež, Prague, Czech Republic, EU, ceccio@ujf.cas.cz
2 CNR-ITAE, Via Santa Lucia sopra contesse, 5 – 98121, Messina (ME), Italy, EU
Conference:
17th International Conference on Nanomaterials - Research & Application, OREA Congress Hotel, Brno, Czech Republic, EU, October 15 - 17, 2025
Proceedings:
Proceedings 17th International Conference on Nanomaterials - Research & Application
Pages:
197-201
ISBN:
978-80-88365-29-7
ISSN:
2694-930X
Published:
27th February 2026
Licence:
CC BY 4.0
Metrics:
2 views
Abstract

Solid electrolytes (SEs) for sodium-based superionic conductors (NaSICON) were first introduced in 1976 and quickly recognized for their excellent ionic conductivity. While considerable effort has been made to develop thin electrolytes for all-solid-state batteries (ASSBs), only a few sodium-based SEs have been successfully fabricated as thin films. These thin films are particularly desirable for their reduced electrical resistance, which typically increases with the thickness of the SE. By reducing the thickness of the SEs to the nanometer scale, their ionic conductivity can be significantly enhanced.In this study, the NASICON composite was initially prepared in the form of pellets using the mixed oxide technique with a planetary ball mill and synthesized by the solid-state method at 1300 °C. The resulting pellets were used as sputtering targets in a low-energy ion facility to prepare continuous NASICON nanofilms. To explore the effect of ion implantation on the electrical properties of NASICON, the prepared films were bombarded with Ni ions at 1.1 MeV and varying fluences, using the Tandetron accelerator at the CANAM infrastructure (NPI Řež). The electrical properties of both the synthesized and implanted films were analyzed through electrochemical impedance spectroscopy (EIS). The results, describing the impact of irradiation on NASICON's properties, are presented here.

Keywords: Energy storage systems, ion beam modifications, nanofilms

© This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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