STRUCTURE AND PROPERTIES OF DLC LAYERS FOR INDUSTRIAL APPLICATIONS

1 MATES Tomáš
Co-authors:
1 LEDINSKÝ Martin 1 VETUSHKA Aliaksei 1 PIKNA Peter 1 FEJFAR Antonín 2 MAREK Aleš 2 VYSKOČIL Jiří 3 ERICHSEN Jörn 3 DAWAH Patrick
Institutions:
1 Institute of Physics AS CR, v.v.i., Cukrovarnická 10, 162 00, Praha 6, Czech Republic, EU
2 HVM Plasma, spol. s r.o., Na Hutmance 2, 158 00 Praha 5, Czech Republic, EU
3 Continental Mechanical Components Germany GmbH, Schorndorfer Str. 91, 93426 Roding, Germany, EU
Conference:
8th International Conference on Nanomaterials - Research & Application, Hotel Voronez I, Brno, Czech Republic, EU, October 19th - 21st 2016
Proceedings:
Proceedings 8th International Conference on Nanomaterials - Research & Application
Pages:
214-219
ISBN:
978-80-87294-71-0
ISSN:
2694-930X
Published:
17th March 2017
Proceedings of the conference were published in Web of Science and Scopus.
Metrics:
20 views / 8 downloads
Abstract

Diamond-like carbon (DLC) layers based on amorphous carbon are used for wide range of applications, mostly for mechanical protection of various industrial components. As the properties of DLC layers are closely linked to their structure, we examined them at micro- and nanoscale by two independent microscopic techniques: Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM) with a good agreement. We compared DLC layers grown on steel substrate and Si wafer and found similarly structured clusters with hundreds of nm in diameter and a certain difference in the density of nucleation centres for each substrate. The measurements of local mechanical properties by the AFM tip revealed that the Si wafer behaves as softer material compared to the growing DLC nanoclusters that also exhibit lower values in the map of the relative local friction coefficient. Finally, we observed changes in the Raman spectra of the DLC exposed to annealing at ambient conditions and found a gradual shift from the diamond phase to the graphite phase as a function of increasing temperature. At the highest temperature of 400°C we observed the formation of tungsten oxide from an additional element contained in the multi-layer stack.

Keywords: DLC, PACVD, AFM, SEM, Raman
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