IN-SITU STUDY OF RECRYSTALLIZATION AND DEFORMATION PROCESSES IN FREE-CUTTING STEEL

1,3 BABINSKÝ Tomáš
Co-authors:
2 DLUHOŠ Jiří 4 CANDEIAS Antoine 3 PETRENEC Martin
Institutions:
1 Brno University of Technology, Faculty of Mechanical Engineering, Brno, Czech Republic, T.Babinsky@seznam.cz
2 TESCAN ORSAY HOLDING, a.s., Brno, Czech Republic, jiri.dluhos@tescan.com
3 fischer Vyškov spol. s r.o., Ivanovice na Hané, Czech Republic, mpetrenec@gmail.com
4 NewTec Scientific, Nimes, France, antoine@newtec.fr
Conference:
27th International Conference on Metallurgy and Materials, Hotel Voronez I, Brno, Czech Republic, EU, May 23rd - 25th 2018
Proceedings:
Proceedings 27th International Conference on Metallurgy and Materials
Pages:
35-39
ISBN:
978-80-87294-84-0
ISSN:
2694-9296
Published:
24th October 2018
Proceedings of the conference were published in Web of Science and Scopus.
Metrics:
66 views / 49 downloads
Abstract

An effect of static recrystallization with inclusion interaction and a change of tensile mechanical properties of drawn free-cutting steel has been studied in the scanning electron microscope (SEM) equipped with a combined in-situ heating and tensile stage. The main goal of all in-situ tests was to effectively improve plasticity and optimize strength which is important for application of the final products from free-cutting steels. The tests were performed on two types of cold-drawn free-cutting steels 11SMnPb30 and a lead-free variant 11SMnBi30. The rough square-shaped bars were delivered in high strength state (Re = 607 MPa, Rm = 658 MPa) and low plasticity (A5 = 10 %) and final fixing products. A series of electron backscattered diffraction (EBSD) mapping of selected area was used for monitoring of static recrystallization process [1-3] on in-situ heated sample from 450 up to 550 °C to provide information about structural changes. The original heavily-deformed structure with many dislocation sub-cells started the recovery process at 450°C and continued to a massive recrystallization at 550 °C. The influence of inclusions on all processes were studied as well. After sample cool down to the room temperature a tensile experiment was performed to compare the change of mechanical properties of the recrystallized sample to the original state of cold-drawn sample without any thermal treatment. A novel approach of multi-site in-situ deformation process monitoring has been used utilizing an advanced software integration and automation possibilities of a combined tensile-heating stage by NewTec and with TESCAN SEM image acquisition.

Keywords: in-situ, scanning electron microscopy, EBSD, materials testing

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