Article Back

ANALYSIS OF CRYSTALLITE SIZE CHANGES IN AN OXIDE LAYER FORMED ON 13CRMO4-5 STEEL USED IN THE POWER INDUSTRY

1 GWOŹDZIK Monika
Institution:
1 Czestochowa University of Technology, Faculty of Production Engineering and Materials Technology, Institute of Materials Engineering, Czestochowa, Poland, EU, e-mail: gwozdzik.monika@wip.pcz.pl
Conference:
27th International Conference on Metallurgy and Materials, Hotel Voronez I, Brno, Czech Republic, EU, May 23rd - 25th 2018
Proceedings:
Proceedings 27th International Conference on Metallurgy and Materials
Pages:
694-699
ISBN:
978-80-87294-84-0
ISSN:
2694-9296
Published:
24th October 2018
Proceedings of the conference were published in Web of Science and Scopus.
Metrics:
401 views / 178 downloads
View Full-text Download PDF
Abstract

The paper presents results of studies on the crystallite sizes of oxide layer formed during a long-term operation on 13CrMo4-5 steel at an elevated temperature (T=470oC, t=190,000h). This value was determined by a method based on analysis of the diffraction line profile, according to a Scherrer formula. The oxide layer was studied on a surface and a cross-section at the outer and inner site on the pipe. X-ray studies were carried out on the surface of a tube, then the layer’s surface was polished and the diffraction measurements repeated to reveal differences in the originated oxides layer.

Keywords: 13CrMo4-5 steel, XRD diffraction, crystallite sizes

© This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

Scroll to Top